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Correlation between Radial Variation and Mechanical Properties of Laminated Veneer Lumber made from 14 Poplar Cultivars Istie RAHAYU, PhD Student Double Degree Indonesia-France Louis DENAUD, Ass. Pr. in Art et Métiers ParisTech, France Remy MARCHAL, Pr., CIRAD, France Wayan DARMAWAN, Pr., in Bogor Agricultural University, Indonesia 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Introduction Materials & methods Results and discussion IUFRO – MEMOWOOD Introduction The veneer processing industry use almost exclusively one poplar cultivar (I-214) for light packaging products. In case of a disease, this could lead to a shortage of raw material or a significant loss in wood quality (Haouzali 2009). Consequently it is necessary to diversify the source of genetic material. Conclusion France is the largest grower of poplar in Europe. It had 236,000 ha (FAO 2008). Total poplar harvesting in 2009 was 1,3 million m3 (FCBA 2011) Istie RAHAYU 2 / 18 IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Introduction (2) Introduction Materials & methods 1) Less lumber defect (knots, cracks and other defects) 2) Stable in dimension and more resistant to warp, twist, bow, and cup; 3) Available in large dimensions Results and discussion Conclusion Istie RAHAYU 3 / 18 2 october 2013 Arts et Métiers ParisTech Centre de Cluny IUFRO – MEMOWOOD Objective Introduction Materials & methods The objectives of this research were to analysed the effect of juvelinity and veneer thickness on mechanical properties in each 14 poplar cultivar Results and discussion Conclusion Istie RAHAYU 4 / 18 IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Sample Preparation Introduction Materials & methods Results and discussion Conclusion Type B : sapwood veneer of 3 mm • Making 7 layer of veneers • Non destructive and destructive test of mechanical properties Type D: false heartwood veneer of 3mm • Making 7 layer of veneers • Non destructive and destructive test of mechanical properties Type E: sapwood veneer of 5,25 mm • Making 4 layer of veneers • Non destructive and destructive test of mechanical properties Type F: false heartwood veneer of 5,25mm • Making 4 layer of veneers • Non destructive and destructive test of mechanical properties Istie RAHAYU 5 / 18 IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny LVL Production Veneer Selection Poplar cultivars : Brenta, Dvina, I-214, Koster, Lambro, Lena, Mella, Soligo, Taro, A4A, Alcinde, Polargo, Trichobel, Triplo Introduction Materials & methods Results and discussion Conclusion From each log, we manufactured two types of panels: - A panel made of "adult" veneer (type B and E); - A panel made of juvenile veneer (from false heartwood - type D and F). We made LVL of 7 layer from 3 mm veneer and 4 layer from 5.25 mm veneer, so that the average thickness of our LVL was 21 mm. All of veneers had already been dried until they reached 8 - 10% of moisture content. Istie RAHAYU 6 / 18 IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Introduction Gluing Process We used PVAc (Poly Vinyl Acetat) as adhesive. The vinyl adhesive that we used was marketed under the name "Rakoll®" _GXL 4. It is in the form of an emulsion and ready for application. We produced 188 LVL panels of 21 mm thickness and 500 mm x 500 mm surface Materials & methods Results and discussion Conclusion Istie RAHAYU 7 / 18 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Introduction Materials & methods Results and discussion IUFRO – MEMOWOOD Preparation Samples for Mechanical Properties Each board was cut into standardized test samples (EN 789), parallel to grain with 10 samples for each board specimens for testing non-destructive characterization and static bending. BING: 3720 (1860 x 2) samples static bending and MOR : 1860 samples The parameter that we used for mechanical properties were Modulus of Elasticity (MOE) and Modulus of Rupture (MOR) computed according to the procedure detailed into the norme EN310. Conclusion Istie RAHAYU 8 / 18 IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Non destructive (BING) and Destructive Test (Instron) Introduction Brancheriau L Materials & methods Results and discussion Conclusion • 4 point bending • Load range of 5000 N at a constant speed 5mm/min until the samples broke • Obtained MOE and MOR Istie RAHAYU 9 / 18 IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Density Introduction Materials & methods Results and discussion Conclusion The equilibrium moisture content was very homogeneous (8.5 ± 0.5%). There was a very good correlation between the densities of LVL made from veneer 3 and 5 mm and densities of solid wood (R2 = 0.81 and 0.78 for 3 and 5 mm subsequently) (Figure top) These results were very satisfactory from the point of view of the homogeneity of the samples that we used in this research. Istie RAHAYU 10 / 18 2 october 2013 Arts et Métiers ParisTech Centre de Cluny IUFRO – MEMOWOOD Modulus of Elasticity (1) Introduction Materials & methods Results and discussion Conclusion (Figure top) showed the correlation between MOE Static and MOE Dynamic for all samples tested (LVL in flatwise and edgewise direction) (1903 samples, 3mm thick veneers). The correlation was excellent (r2 = 0.93). This indicated that BING was a reliable non destructive instrument for mechanical grading Poplar based on MOE. It was correspondence with Haouzali (2009), noticed the same relationship between dynamic and static module of Poplar LVL (correlation coefficient (r) of the regression is 0.88 and the determination coefficient (r2) is 0.77, with highly statically significant at the 1% level). It was also shown that the dynamic MOE is always slightly higher than the static MOE. The resonance method is interesting to predict stiffness which is often penalizing poplar form mechanical classment. Industrial control plywood and LVL boards could be possible with BING method (Haouzali 2009). Istie RAHAYU 11 / 18 IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Introduction Materials & methods Results and discussion Conclusion MOE (2) The MOE values that we used were the average values from LVL made from 3 mm and 5 mm veneers in flatwise and edgewise bending test. The results were very well correlated with MOE of solid wood (Figure Top), in line with Haouzali (2009) However, as Haouzali (2009) observe it, the MOE of LVL were generally lower than the MOE of solid wood. Thus, for the LVL, there were cultivars with high rigidity values (Lambro, Brenta, Taro, Alcinde, Soligo, Lena, Koster) and three cultivars (I214, A4A and Triplo) were unsuitable for structural applications (Figure Down). Istie RAHAYU 12 / 18 2 october 2013 Arts et Métiers ParisTech Centre de Cluny IUFRO – MEMOWOOD Modulus of Rupture (MOR) Introduction Materials & methods Results and discussion Conclusion The comparison of the MOR values between LVL and solid wood also showed a good correlation. The effect of lamination combined with adhesive performed significantly improved the MOR of these cultivars (about 20% on average compared to solid wood) The poplar LVL and plywood proprieties can be influenced considerably by the cultivar, the glue type and the veneer thickness (Haouzali 2009). Istie RAHAYU 13 / 18 2 october 2013 Arts et Métiers ParisTech Centre de Cluny IUFRO – MEMOWOOD Effect of Radial Position Introduction Materials & methods Results and discussion Conclusion Istie RAHAYU 14 / 18 IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Introduction Materials & methods Results and discussion Conclusion Effect of Radial Position The advantage of using veneers taken from sapwood , and therefore supposed to be less juvenil than heartwood, is obvious since the mechanical properties are much better (between 14 to 21%) for a comprarble density (Table down). This proved that there was an effect due to juvelinity in every poplar cultivar. It also showed that LVL from 5 mm veneers had the highest increase percentage from juvenile to mature in MOE dynamic, MOE quasistatique MOR and density, 16%, 18%, 21% and 2% subsequently. Mean Value of 14 Poplar Cultivars LVL 5 mm Mature Juvenile gain in % LVL 3 mm Mature Juvenile gain in % MOE dynamique (MPa) 9429 8126 MOE quasistatique (MPa) 9129 7737 +16 MOR (Mpa) Density (kg/m3) 54 45 400 390 +18 +21 +2 9259 8193 8769 7629 56 48 417 412 +13 +15 +16 +1 Istie RAHAYU 15 / 18 IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Conclusion • BING, was reliable instrument for estimating MOE from destructive test. Some cultivars have a real potential for structural applications (Lambro, Soligo, Alcinde, Brenta and Taro) while others could be excluded (A4A, I-214, Triplo). Introduction Materials & methods Results and discussion Conclusion • All cultivars could be well peeled and presents an excellent peelability as [NURBAITY.2012]. General cutting conditions used for I214 were applied for the 14th cultivars. • There was significant variation sapwood to heartwood (supposed mature to juvenile wood) for each cultivar. The difference of mean MOE and mean MOR between juvenile and mature LVL were 15% and 17% for an increase of density of 1%. Finally, the use of thicker veneers reduced the use of adhesive, simplified and accelerated the production of panels without altering their mechanical properties. Istie RAHAYU 16 / 18 IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Introduction Materials & methods Results and discussion Conclusion References [CRPF]. 2013. Bilan du programme de restitution TRANSPOP 2 (programme transfrontalier entre les régions Nord Pas de Calais - Picardie et la Belgique sur le peuplier), présenté mercredi 5 décembre 2012 Denaud LE. 2006. Analyses vibratoires et acoustiques du déroulage [Tesis]. Cluny: Sciences des Métiers de l’Ingénieur, Arts et Métiers. Haouzali EH. 2009. Effets cultivar et station sur les propriétés mécaniques de LVL et contreplaqués issus du déroulage de peupliers [Tesis]. Cluny: Sciences des Métiers de l’Ingénieur, Arts et Métiers Haouzali EH, Marchal R, Bleron L, Butaud JC. 2010. Effets cultivar et stations sur la déroulabilité du peuplier et la qualité des produits issus du déroulage (dossier: qualités du bois de peuplier). Forêt entreprise. 191: 22-26 Kretschmann DE, Moody RC, Pellerin RF, Bendtsen BA, Cahill JM, McAlister RH & Sharp DW. 1993. Effect of Various Proportion of Juvenile Wood on Laminated Veneer Lumber. Forest Product Laboratory Research Paper FPL-RP-521. Kretschmann DE, Alden HA & Verrill S. 1997. Variation of Microfibril Angle in Loblolly Pine Comparison of Iodine Crystallization and X-Ray Diffraction Technique. The Proceeding of The IAWA/IUFRO International Workshop on The Significance of Microfibril Angle to Wood Quality. Westport, New Zealand. Nurbaity. 2012. Etude de la déroulabilité de 14 cultivars de peupliers : Analyse des efforts de coupe et de l’état de surface des placages . MASTER STVE Sciences et Technologies du Vivant et de l’Environnement, Mention Aliments et bioproduits, Nutrition, Santé, Spécialité BF2E Bois, Fibres, Énergie, Environnement Istie RAHAYU 17 / 18 Thank You – Merci Beaucoup – Terima Kasih Any Questions ? Doctorants LaBoMaP IUFRO – MEMOWOOD 2 october 2013 Arts et Métiers ParisTech Centre de Cluny Density Introduction Materials & methods Results and discussion Conclusion The equilibrium moisture content was very homogeneous (8.5 ± 0.5%). There was a very good correlation between the densities of LVL made from veneer 3 and 5 mm and densities of solid wood (R2 = 0.81 and 0.78 for 3 and 5 mm subsequently) (Figure top) These results were very satisfactory from the point of view of the homogeneity of the samples that we used in this research. The observed discrepancy between the densities of LVL 3 and 5mm was systematic (intercept of linear regressions difference about 50 kg/m3) and mainly due to the removal of three glue line between the two lay up. They were about 30 kg/m3 because the weight adhesive application was about 200 g/m². Istie RAHAYU 19 / 18