Influencing Factors and Parameters in the Extrusion Process
Transcription
Influencing Factors and Parameters in the Extrusion Process
MASCHINEN UND ANLAGEN MACHINERY AND EQUIPMENT Influencing factors rubber extrusion pin type extruder extruder performance material outlet temperature extrudate quality The performance of an extruder aggregate as a result of the maximum permitted screw speed is limited by the maximum permitted material outlet temperature or by the required level of homogeneity in the extrudate. As a basic result of fundamental trials both the material outlet temperature as well as the level of reached homogeneity is corresponding to the duration time for the compound to stay inside the extruder and the effective shearing rate. This is mostly being determined by the back pressure depending on the profile size and the compound properties and by the screw design or special installed shearing elements like pins. Further important influencing factors, which may influence the performance of up to 30 % or even more, are the production conditions such as TCU-settings for screw, barrels and head, and the pin configuration. Einflussfaktoren und Parameter auf den Extrusionsprozess Einflussgrößen Kautschukextrusion Stiftextruder Ausstoßleistung Materialaustrittstemperatur Extrudatqualität Die Leistungsfähigkeit eines Extruders und damit die zulässige Schneckendrehzahl wird begrenzt durch die maximal zulässige Materialaustrittstemperatur oder durch die geforderte Produktqualität, bestimmt durch den erreichten Homogenisierungsgrad im Extrudat. Erkenntnisse aus Grundlagenuntersuchungen hierzu zeigen, das sowohl die Materialaustrittstemperatur als auch der erreichte Homogenisierungsgrad von der Verweildauer der Kautschukmischung im Extruder und vom Grad ihrer Scherung abhängt. Diese wiederum werden bestimmt von dem von der Profilgröße und den Mischungseigenschaften abhängigen Gegendruck, der Schneckengeometrie und der Effektivität eventuell vorhandener Scherelemente wie z. B. Stiften. Weitere wichtige Einflussgrößen, die die Leistungsfähigkeit bis zu 30 % oder mehr beeinträchtigen können, sind außerdem die Betriebsbedingungen wie Temperierung von Schnecke, Zylindern und Kopf und die Wahl Bestiftung. 362 Influencing Factors and Parameters in the Extrusion Process Even if extruder size and configuration as well as the screw design are important factors for the performance and the product quality of an extrusion line, there are other influencing factors such as compound properties, profile size (back pressure), screw speed, TCU-settings and pin configuration, which mainly influence the actual production and which have to be taken into consideration for optimisation of the extrusion process individually. Therefore modern extrusion lines are supplied with computer based memories in which the optimised production data are stored as recipes for different profiles and compounds and can individually be recalled for the corresponding application. These production data have of course at first to be optimised for each single profile due to the actual requirements as productivity, material temperature and appearance according to the performance triangle of the extrusion shown in Fig. 1. The extruder output is the main determining factor for the productivity. It is first of all determined by the extruder size, the screw speed and the back pressure, i.e. the profile size. But on the other hand the output is also limited either by the permitted material outlet temperature or by the required quality of the extrudate, i.e. the surface appearance or product homogeneity. The target of the optimising process is to find the right combination of the parameters for max. output at lowest material outlet temperature and sufficient appearance. to reduce the shearing rate and the material outlet temperature on the expense of output. Of course the existing diagram may have to be modified according to other influencing factors such as compound type, consistence and properties, profile size and others. Extruder performance diagram ML(1þ4) 100 8C Fig. 2 shows the performance of ThyssenKrupp pin type extruders, i.e. the output [kg/h] of different extruder sizes depending on the screw speed [rpm]. Parameters are the additionally included estimated material outlet temperature graphs. According to the graphs it is shown, that higher screw speed does not only increase the output, but also the material outlet temperature is increased because of additional shearing of the compound. Exceeding the permitted temperature will then require reduction of the screw speed Compounds with high Mooney-viscosity normally cause high torque because of high flow resistance inside both the flow channels of the screw and the extrusion Influence of back pressure The actual back pressure in the extrusion head determines the actual operational point of the screw, i.e. the actual output of the entire extruder aggregate. It is depending on the profile size, the design of the flow channels, the actual viscosity of the compound (depending on the actual material temperature) and the flow conditions (temperature of the extrusion head). Small profiles, long flow channels, high compound viscosity and low extrusion head temperatures cause high back pressure and low output as well as high material temperature. The influence of back pressure on output and material outlet temperature is shown in Fig. 3, in which the different back pressure levels are realized by using different profile sizes: Influence of the compound The influence of the compound properties on material temperature and output is mainly characterized by the visco-elastic behaviour of the compound, expressed by the Mooney-viscosity L. Köster, Hamburg-Harburg Corresponding author: Dr.-Ing. Lothar Köster ThyssenKrupp Elastomertechnik GmbH Seevestr. 1 21079 Hamburg-Harburg Tel.: 0 40/7 71 79-0 KGK Kautschuk Gummi Kunststoffe 58. Jahrgang, Nr. 7-8/2005 Fig. 1. Performance triangle of extrusion the material inside the extruder and to reduce the number of shearing elements like pins, if low material temperature is wanted. On the other side especially homogeneitycritical compounds like natural rubber (NR) may require a high grade of shearing for good plastification and homogenizing to get good appearance. This will either need special shearing elements like e.g. a high number of pins or special screw design, or it can be influenced by selecting a TCU-setting, which reduces the output for a longer time of duration of the material inside the extruder. High output means low duration time for the material inside the extruder, i.e. low shearing rate, low level of uniformity and low material outlet temperature. Low output means longer duration time for the material inside the extruder, i.e. high shearing rate, high level of uniformity and homogeneity, but also higher material outlet temperature. The influence of different TCU-settings due to their effect on output and material outlet temperature is shown in Fig. 5. A guideline for correct TCU-settings according to required output and material outlet temperature or product quality is shown in following list: Influence of pin configuration Fig. 2. Extruder performance diagram head. Therefore a high level of shearing is needed. This causes high material temperatures and, corresponding hereto, a reduced output according to the graph in Fig. 4. Low material temperature always means, that the compound needs to be sheared in a low range only. Corresponding hereto it is necessary to reduce the duration for According to a.m. statements the number of pins in a pin type extruder is of important influence as well for output, i.e. productivity, as also for shearing and plasticizing of the compound, i.e. product quality. A great number of pins will always increase the shearing rate and by that give good homogeneity and appearance. But it will also increase the material temperature. Influence of TCU-settings The simplest and therefore most important possibility for the operator to influence as well the product quality as also the output is given by changing the TCU-settings according to the requirements of the compound. But since rubber is a bad heat conductor it is a mistake to believe, that the material temperature can be influenced by cooling the extruder or the extrusion head to draw out the internal heat of the rubber. But instead of it is possible to influence the adhesion between material and barrel or flow channel walls by selecting the correct temperature. Fig. 3. Influence of back pressure KGK Kautschuk Gummi Kunststoffe 58. Jahrgang, Nr. 7-8/2005 363 On the other hand a low number of pins will reduce the shearing rate and by that reduce the material temperature. But on the other hand the result may be an insufficient homogeneity and insufficient appearance, especially for homogeneity-critical compounds like natural rubber. The target of starting up an extrusion line therefore is to find the lowest necessary number of pins to achieve as low a material outlet temperature as possible and at the same time to achieve an acceptable surface appearance. Fig. 6 shows the effect of different pin configurations on a KGS 150/16 pin type extruder on output and material outlet temperature: Fig. 4. Influence of different Mooney-viscosity Influence of screw design Fig. 5. Influence of different TCU-settings on output and material temperature Since shearing rate and duration time inside the extruder on one hand increase the product quality because of increased homogeneity and uniformity, it on the other hand also will increase the material outlet temperature and so limit the productivity. To reduce the shearing rate but still to have the effect of good mixing and uniformity ThyssenKrupp Elastomertechnik developed a new series of high performance screws with improved shearing and mixing zones by flight separation in the pin section of the screw as shown in Fig. 7. The separation of the flights and the flow channels in the pin section of the screw continuously distributes and collects the flow of the compound and mix the different flows for good uniformity without additional shearing. By that for the same or even better level of uniformity and product quality the number of pins may be reduced, so that either the material outlet temperature will be decreased or the screw speed might be increased for more output at same temperature. A comparison of the output / temperature relationship between 2 similar pin type screws KGS 150/16 with/without flight separation is shown in Fig. 8. Summary According to a.m. comments regarding the different influence factors and operational conditions and there influence on productivity and product quality of an extrusion process, it can be stated, that each application and each product normally require its own optimisation due to the compound and production requirements. Fig. 6. Influence of pin configuration 364 KGK Kautschuk Gummi Kunststoffe 58. Jahrgang, Nr. 7-8/2005 List 1. Guideline TCU-Settings for TKEL-Pin Type Extruders Screw Inlet Barrel Pin Barrel 1 Pin 2 þ Ext. Head High Output Low Temperature 90 – 95 8C 20 – 30 8C 40 8C 60 8C 90 – 100 8C Low Output Good Homogeneity 70 – 80 8C 40 – 50 8C 60 – 70 8C 80 – 90 8C 90 – 100 8C Fig. 7. High output pin type screw KGS 150/16 with flight separation The qualified operator has a number of different possibilities to his disposal to optimise the process and to get best results. On the other hand, unqualified operation may lead to losses or scrap production, which normally are not in the responsibility of the machine. But anyway, no extruder or extrusion line, even when it is operated by the most qualified operator, can compensate problems in the process, which are caused by insufficient compound. The result of any extrusion process is a combination of all the influencing factors, starting with the quality of the ingredients and the consistence and properties of the compound, continuing with the qualification of the operators and the operational conditions and ending with the performance of the extruders and the entire extrusion line. Only when all these parameters are taken into consideration and respected, the result can be a good tire. The author Dr.-Ing. Lothar Köster ist Leiter der Verfahrenstechnik / Extrusion bei der Firma ThyssenKrupp Elastomertechnik GmbH, Hamburg-Harburg. Fig. 8. Output / temperature relationship with/without flight separation KGK Kautschuk Gummi Kunststoffe 58. Jahrgang, Nr. 7-8/2005 365